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正交设计研究金菊花总提物及总黄酮提取工艺
引用本文:彭少平,李竣,芦金清.正交设计研究金菊花总提物及总黄酮提取工艺[J].湖北中医学院学报,2002,4(2):29-30.
作者姓名:彭少平  李竣  芦金清
作者单位:湖北中医学院430061
摘    要:目的:探讨金菊花总提物,总黄酮提取工艺。方法:采用正交设计法。结果:浸膏最佳提取工艺为A3B3C1,即60%乙醇5倍量回流2小时,共提取2次;总黄酮最佳提取工艺诬蔑国A3B3C2,即60%乙醇5倍量加流1小时,共提取2次。考察结果显示:按A3B3C1浸膏得率可达47.81%。按A3B3C2总黄酮溶出量可达4.37%。结论:乙醇浓度和回流时间对浸膏得率及总黄酮溶出量有较大影响。应加以控制。

关 键 词:神农金菊花  总黄酮  提取工艺  正交设计  浸膏得率
文章编号:1008-987X(2002)02-0029-02
修稿时间:2002年1月21日

Study on Extracting Technology of Total Extraction and Total Flavone in Dendranthema.Morifolium Tzvel with Orthogonal Design
Peng Shaoping,Li Jun,Lu Jinqing Hubei College of Traditional Chinese Medicine,Wuhan.Study on Extracting Technology of Total Extraction and Total Flavone in Dendranthema.Morifolium Tzvel with Orthogonal Design[J].Journal of Hubei College of Traditional Chinese Medicine,2002,4(2):29-30.
Authors:Peng Shaoping  Li Jun  Lu Jinqing Hubei College of Traditional Chinese Medicine  Wuhan
Affiliation:Peng Shaoping,Li Jun,Lu Jinqing Hubei College of Traditional Chinese Medicine,Wuhan 430061
Abstract:To seek the optimum extracting technology of total extraction and total flavone of Dendranthema. morifolium Tzvel. Methods: The orthogonal design was used. Results:The optimum extracting condition of total extraction was A 3B 3C 1,that is adding five times amount of 60% alcohol and refluxing and extracting for 2h(totally extracting for 2 times); the optimum extracting condition of total flavone was A 3B 3C 2, that is adding five times amount of 60% alcohol and refluxing and extracting for 1h (totally extracting for 2 times). The total extraction and total flavone could raised to 47 81% and 4 27%.Conclusion:The alcohol concentration and the time of refluxing should be strictly controlled because of the large influence on the dissolution of total extraction and total flavone.
Keywords:Dendranthema  morifolium Tzvel  Total flavone  Orthogonal design  Extracting technology
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